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1 article(s) from Vlasenko, Yulia A

Thermal stability of N-heterocycle-stabilized iodanes – a systematic investigation

Andreas Boelke,
Yulia A. Vlasenko,
Mekhman S. Yusubov,
Boris J. Nachtsheim and
Pavel S. Postnikov

Beilstein J. Org. Chem. 2019, 15, 2311–2318, doi:10.3762/bjoc.15.223

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Graphical Abstract

Figure 1: General structure of aryl-λ³-iodanes.

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Figure 2: T_peak and ΔH_dec-values for a range of N- and O-substituted iodanes.

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Figure 3: TGA/DSC curves of (a) benziodoxolone 1, (b) triazole 2 and (c) pyrazole 6.

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Figure 4: Decomposition enthalpy (ΔH_dec) scale for pseudocyclic tosylates 1–15 and cyclic iodoso species 16 a...

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Figure 5: Correlation between the relative reactivity for pseudocyclic NHIs based on the reaction time in the...

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Figure 6: T_peak and ΔH_dec values for a range of N- and O-substituted iodanes.

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Figure 7: Decomposition enthalpy (ΔH_dec) scale for (pseudo)cyclic mesitylen(phenyl)- λ³-iodanes 18–33.

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Figure 8: TGA/DSC curves for the benzimidazole based diaryliodonium salt 25.

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Figure 9: TGA/DSC curves for the cyclic triazole 32.

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Scheme 1: The thermal decomposition of (pseudo)cyclic N-heterocycle-stabilized mesityl(aryl)-λ³-iodanes 25 an...

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Published 27 Sep 2019

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